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91.
The effect of preparation method on MnO
x
–CeO2 mixed oxide catalysts for methane combustion at low temperature was investigated by means of BET, XRD, XPS, H2-TPR techniques and methane oxidation reaction. The catalysts were prepared by the conventional coprecipitation, plasma and
modified coprecipitation methods, respectively. It was found that the catalyst prepared by modified coprecipitation was the
most active, over which methane conversion reached 90% at a temperature as low as 390 °C. The XRD results showed the preparation
methods had no effect on the solid solution structure of MnO
x
–CeO2 catalysts. More Mn4+ and richer lattice oxygen were found on the surface of the modified coprecipitation prepared catalyst with the help of XPS
analysis, and its reduction and BET surface area were remarkably promoted. These factors could be responsible for its higher
activity for methane combustion at low temperature. 相似文献
92.
93.
目的:对肿节风注射液进行异常毒性、溶血与凝聚试验、过敏反应安全性实验评价。方法:根据《中国药典》2010年版一部附录"中药注射剂安全性检查法应用指导原则"的要求及相关项目的技术规范进行试验。结果:按每只小鼠尾静脉注射0.5ml肿节风注射液,结果实验小鼠均无异常反应;溶血与凝聚试验供试品管中的溶液在3小时内不发生溶血和凝聚;按豚鼠腹腔注射0.5ml/只和静脉注射1.0ml/只作为本品的致敏剂量和激发剂量,结果试验豚鼠均未出现过敏反应。结论:本肿节风注射液进行的异常毒性、溶血与凝聚试验和致敏反应的安全性评价符合规定。 相似文献
94.
Asymptotic state behaviour and its modeling for saturated sand 总被引:3,自引:0,他引:3
A new double hardening elasto-plastic model is proposed in this paper based on the existing unified hardening model (UH model).
By assuming that there is part coupling effect between the plastic volumetric strain and plastic shear strain, hardening parameters
consisting of a coupled and an uncoupled components are adopted in this model. A unique feature of this model is that it can
describe not only the conventional drained and undrained behaviors of soil, but also the stress-strain relationships of soil
under partially drained conditions which can be volumetric compression or dilation. Adopting the asymptotic state concept,
simple equations for estimating the limiting stress ratio under undrained or earth pressure at rest (i.e. K
0) conditions are derived. The new model is relatively simple to be adopted in practice for two reasons. First, the same soil
parameters as in Cam-clay model are used except the addition of one extra parameter, the stress ratio at the characteristic
state. Second, all the parameters can be determined using conventional triaxial compression tests.
Supported by the National Natural Science Foundation of China (Grant Nos. 10672010 and 50479001) and the National Earthquake
Science Item (Grant No. 200808076) 相似文献
95.
Jinguang?Xu Zhijian?TianEmail author Junwei?Wang Yunpeng?Xu Zhusheng?Xu Liwu?Lin 《Korean Journal of Chemical Engineering》2003,20(2):217-221
Hydrothermal synthesis by using urea hydrolysis at 1.0-3.0 MPa and 120-130 ‡C was employed to prepare Mn-substituted hexaaluminate
catalysts for methane combustion. The results from DTA-MS demonstrated that CO3- and Off anions co-exist in the hydrothermal reaction. XRD reveals that the components of carbonates and hydroxides in the
hydrothermal reaction are more favorable than those in the (NH4)2CO3 co-precipitation for the formation of the Mn-substituted hexaaluminate phase. After calcination at 1,200 ‡C for 2 h, LaMnAl11O19 is the major phase of the catalyst prepared by the hydrothermal synthesis method while LaAlO3 is the major one of the catalysts prepared by NH4OH and (NH4)2CO3 co-precipitation. The catalyst prepared by hydrothermal synthesis has higher activity than that prepared by NH4OH and (NH4)2CO3 co-precipitation. The major reason is that more Mn2+ ions have incorporated into the hexaaluminate lattice. The effect of drying methods on the formation of hexaaluminate phase
was also discussed. 相似文献
96.
Michail V. Kozlov Junwei Zhu Peter Philipp Wittko Francke Elena L. Zvereva Bill S. Hansson Christer Löfstedt 《Journal of chemical ecology》1996,22(3):431-454
The fifth abdominal segment of femaleEriocrania semipurpurella (Stephens) andE. sangii (Wood) contains a pair of exocrine glands. Hexane extracts of this segment were prepared from both species and analyzed by gas chromatography with simultaneous flame ionization and electroantennographic detection (EAD). For both species, the EAD active peaks were identified as nonan-2-one, (Z)-6-nonen-2-one, and (Z)-6-nonen-2-ol by means of mass spectrometry and comparison of retention indices with those of synthetic standards. Enantiomeric separation of chiral alcohols from the female extracts was achieved by gas chromatographic analysis on a cyclodextrin column. InE. semipurpurella, a mixture of (2S,6Z)-nonen-2-ol and (2R,6Z)-nonen-2-ol (2: I) was found, whereas inE. sangii (2S,6Z)-nonen-2-ol was the predominant enantiomer and only traces of theR enantiomer were indicated by the antennal response. In field tests, a blend of the three compounds was not attractive to conspecific males. A subtractive assay showed that the alcohol in various enantiomeric mixtures was the only attractive compound, whereas addition of (Z)-6-nonen-2-one to the alcohol completely inhibited the attraction of both species. A trapping experiment including a wide range of ratios between theR andS enantiomers showed that baits containing 95–100% of theS enantiomer were attractive to maleE. sangii, whereas males ofE. semipurpurella were attracted to all tested ratios of the enantiomers. However, the response profiles of maleE. semipurpurella differed between populations from southern Sweden, south Finland, and the Kola Peninsula in Russia. In south Sweden males were maximally attracted to a racemic mixture of the alcohols. At the Kola PeninsulaE. semipurpurella was attracted to baits containing 95–100% of theR enantiomer. In south Finland all tested ratios between 0 and 100%R enantiomer trappedE. semipurpurella, but the trap catches appeared to be bimodally distributed with peaks around 15 and 70%R enantiomer. The trapping results suggest the existence of pheromone races or sibling species among the specimens identified asE. semipurpurella.Dedicated to Prof. H. J. Bestmann on the occasion of his 70th birthday. 相似文献
97.
98.
This paper proposes a novel relay selection strategy based on the feedback beamforming (BF) information through designed sector sweep (SSW) report frame for millimeter-wave (mmWave) wireless personal networks (WPANs). First, an SSW report frame compatible with IEEE 802.11ad standard is designed. Second, an approach collecting instantaneous channel state information (CSI) overheard during BF is devised. Third, with the aim of minimizing the outage probability and maximizing the overall network throughput capacity, the optimal relay selection issue for non-line-of-sight (NLoS) links is formulated as a bipartite graph, and Kuhn Munkres (KM) algorithm is provided to resolve it. Both theoretical analysis and simulation results show, with CSI considering NLoS conditions and selected relays according to the overall network throughput capacity maximization principle, the improvements achieved over opportunistic relay selection strategy in terms of overall network throughput capacity and outage probability with minimal modifications to IEEE 802.1lad. 相似文献
99.
In this paper, a broadband dielectric resonator antenna (DRA) with a simple H‐slot feeding structure is proposed. The broad bandwidth (~45%) and uni‐directional radiation enable this DRA suitable to work as a radiation element in the construction of a beam‐scanning array with not only low frequency sensitivity which is important for accurate angle estimation of in‐coming targets, but also a wide scanning range. Moreover, stable coupling coefficients are established around all the above three resonances with respect to its corresponding feeding line, ensuring a low sidelobe level (SLL) across the whole operating frequency range. In order to realize such a DRA, a latticed rectangular structure is utilized to generate the lower two resonances, while the upper resonance is generated by its H‐shaped feeding slot. The shape of the latticed dielectric resonator is also modified according to a 3‐D printed fixing structure for an accurate installation. A 20‐element beam‐scanning prototype is demonstrated and manufactured. The range of scanning angle is from ?36° to +13° within the bandwidth of 10 to 16 GHz, corresponding to a frequency sensitivity of only 122.5 MHz/o. The achieved SLL are smaller than 19 dB for all scanning beams. The above performance indicates that, this array is very suitable for near‐range radar systems requiring an accurate angle estimation. 相似文献
100.